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The development of cesium selective adsorbent is urgent subject for the decontamination of intermediate and high level water from nuclear facilities especially in nuclear accidents. For the selective adsorption and stable immobilization of radioactive cesium, K-Ni- hexacyanoferrate (II) loaded zeolite (FCzeolite) (synthesized zeolite of Hanoi University of Science and Technology) were prepared by impregnation/precipitation method. | The study on preparing absorbent of potassium nickel hexacyanoferrate (II) loaded zeolite for removal of cesium from radioactive waste solutions and stable solidification method for those spent absorbents