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In this article, we have reported the synthesis procedure of VO2 nanorods and micro/nano urchin-like VO2 structure and evaluating the methylene blue (MB) adsorption properties. Morphology and particle size of VO2 were observed by FE-SEM. The phase formation of VO2 was studied by XRD. Raman spectroscopy was also used for characterization of VO2. | Synthesis of micro/nano urchin-like VO2 particles and its decolorization of methylene blue