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(BQ) Part 2 book "Analytical chemistry handbook" has contents: Mass spectrometry, radiochemical methods, magnetic susceptibility, electroanalytical methods, thermal analysis, refractometry, elemental analysis of organic compounds,.and other contents. | Source: DEAN’S ANALYTICAL CHEMISTRY HANDBOOK SECTION 10 MASS SPECTROMETRY 10.1 INSTRUMENT DESIGN Figure 10.1 Components of a Mass Spectrometer 10.1.1 Inlet Sample Systems 10.2 IONIZATION METHODS IN MASS SPECTROMETRY 10.2.1 Electron Ionization 10.2.2 Chemical Ionization 10.2.3 Other Ionization Methods 10.3 MASS ANALYZERS 10.3.1 Magnetic-Deflection Mass Analyzer 10.3.2 Double-Focusing Sector Spectrometers 10.3.3 Quadrupole Mass Analyzer 10.3.4 Time-of-Flight Spectrometer Figure 10.2 Quardrupole Mass Analyzer 10.3.5 Ion-Trap Mass Spectrometer 10.3.6 Additional Mass Analyzers 10.3.7 Resolving Power 10.4 DETECTORS 10.4.1 Electron Multiplier 10.4.2 Faraday Cup Collector 10.5 CORRELATION OF MASS SPECTRA WITH MOLECULAR STRUCTURE 10.5.1 Molecular Identification 10.5.2 Natural Isotopic Abundances Table 10.1 Isotopic Abundances and Masses of Selected Elements 10.5.3 Exact Mass Differences 10.5.4 Number of Rings and Double Bonds 10.5.5 General Rules 10.5.6 Metastable Peaks 10.6 MASS SPECTRA AND STRUCTURE 10.6.1 Initial Steps in Elucidation of a Mass Spectrum 10.6.2 General Rules for Fragmentation Patterns 10.6.3 Characteristic Low-Mass Fragment Ions 10.6.4 Characteristic Low-Mass Neutral Fragments from the Molecular Ion Table 10.2 Mass Spectra of Some Selected Compounds 10.7 SECONDARY-ION MASS SPECTROMETRY 10.8 ISOTOPE-DILUTION MASS SPECTROMETERY (IDMS) 10.9 QUANTITATIVE ANALYSIS OF MIXTURES Table 10.3 Mass Spectral Data (Relative Intensities) for the C1 to C3 Alcohols 10.10 HYPHENATED GC-MS AND LC-MS TECHNIQUES 10.10.1 GC-MS 10.10.2 LC-MS Bibliography 10.2 10.2 10.2 10.3 10.3 10.3 10.4 10.4 10.5 10.5 10.5 10.5 10.6 10.6 10.7 10.7 10.7 10.7 10.8 10.8 10.8 10.8 10.8 10.9 10.10 10.10 10.10 10.11 10.11 10.11 10.12 10.12 10.13 10.23 10.24 10.24 10.25 10.26 10.26 10.27 10.28 10.1 Downloaded from Digital Engineering Library @ McGraw-Hill (www.digitalengineeringlibrary.com) Copyright © 2004 The McGraw-Hill Companies. All rights reserved. Any use is subject to the Terms of Use as
